Boiling Point (°C) 0 - 100 (15) 101 - 200 (7) Melting Point (°C) less than 0 (1) 0 - 100 (7) 101 - 200 (2) 201 - 300 (1) Reaction Suitability. Structure of CH 3 MgCl(thf) 2, which is representative of the species in donor solvents. To methylmagnesium chloride [from the action of gaseous methyl chloride on 121.5 gm (5 moles) of magnesium in 1600 ml of dry di-n-butyl ether] is added 610 ml (5 moles) of tert-amyl chloride in 1 liter of di-n-butyl ether at 5°C over a period of 8 hr.
Methylmagnesium chloride (20% solution in tetrahydrofuran) for synthesis - Find MSDS or SDS, a COA, data sheets and more information. Decomposition with ice and distillation of the ether yielded the crude product at bp 37°−50°C. Silylations. Quality Level 200: vapor pressure 200 hPa ( 20 °C) autoignition temp. Boiling Point : N/A : Density : 1.013 g/mL : Solubility in H2O : N/A : Exact Mass : 73.977369 : Monoisotopic Mass ... Methylmagnesium Chloride is a Grignard reagent, available as a standard 3.0 M (22 wt %) solution in THF; custom concentrations and forms are also available. Methylmagnesium chloride: EINECS: 211-629-7 CAS No. 215 °C (THF) expl. AKOS009159222. Question? Available on GSA Contract (1) Greener Alternative (1) Available for Sale. CH3MgI. Feature. Properties. General information; Classification & Labelling & PBT assessment; Manufacture, use & exposure; Physical & Chemical properties ; Environmental fate & pathways; Ecotoxicological information; Toxicological information; Analytical methods; Guidance on safe use; Assessment reports; Reference substances; GHS; DSD - … 676-58-4: Density: 1.013 g/mL at 25 °C Solubility: reacts with water Melting Point: Formula: CH3 Cl Mg Boiling Point: 66 °C Molecular Weight: 74.79 Flash Point?1 °F Methylmagnesium chloride (20% solution in tetrahydrofuran) for synthesis Synonym: Chloromethylmagnesium Purchase; Safety & Documentation; Protocols & Articles; Peer-Reviewed Papers ; Related Products; Purchase. SCHEMBL1072. EC number: 211-629-7 | CAS number: 676-58-4 . KS-00000WDY.
Methylmagnesium iodide solution, 3.0 M in diethyl ether. Methylmagnesium chloride. Methylmagnesium iodide 3M solution in DEE Pricing > SDS > Data Sheet > WHOLESALE/SKU 0000-742-255539 . Relative to the more commonly encountered methylmagnesium bromide and methylmagnesium iodide, methylmagnesium chloride offers the advantages of low equivalent weight and low cost. AUPXBVDHVRZMIB-UHFFFAOYSA-M. ACN-S001882. (Trimethylsilyl)methylmagnesium Chloride Solution: MG-OMX-01-SOL .
lim. It is prepared by the reaction of methyl chloride and magnesium in ethyl ether. Acylations. USA; Globally; Search term: "Trimethylsilyl chloride" Compare Products: Select up to 4 products.